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My thinking was that there are 1 and 2 in ethyl by the oxygen, 3 off the 1st carbon of the aromatic group near the oxygen, 4 from the four points in the aromatic ring, 5 in the opposite carbon of the aromatic group by the ketone, and then 6 off the ketone Title: NMR Practice Problems (Solutions) Author: Dr. Laurie S. Starkey Created Date: 4/10/2014 10:24:48 PM Spectroscopy worksheet. Solving Spectroscopy Problems: Putting it All Together Once you’ve analyzed the mass spectrometry, infrared spectrometry, 1H‐NMR, and 13C‐ NMR data, there is no one way to put them together. Carbon 13 NMR Problems 1 Organic Chemistry Dr Sundin. Determine the structure of the six compounds whose IR and PMR spectra are provided on the attached sheets, given the following comments about the provided information and spectra. Organic Chemistry Practice Problems At Michigan State. 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